Information card for entry 4102237

Structure parameters

• Formula: C55 H40 B F20 N2 Pd
• Calculated formula: C55 H40 B F20 N2 Pd
• Title of publication: Cationic Polymerization and Insertion Chemistry in the Reactions of Vinyl Ethers with (α-Diimine)PdMe+ Species
• Authors of publication: Changle Chen; Shuji Luo; Richard F. Jordan
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 5273 - 5284
• a: 15.922 ± 0.003 Å
• b: 20.076 ± 0.004 Å
• c: 19.176 ± 0.003 Å
• α: 90°
• β: 121.573 ± 0.01°
• γ: 90°
• Cell volume: 5222.3 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0435
• Weighted residual factors for significantly intense reflections: 0.0972
• Weighted residual factors for all reflections included in the refinement: 0.1042
• Goodness-of-fit parameter for all reflections included in the refinement: 0.982
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No