Information card for entry 4102395

Structure parameters

• Formula: C45 H55 Ni2 P2
• Calculated formula: C45 H55 Ni2 P2
• Title of publication: Synthesis and C-C Coupling Reactivity of a Dinuclear NiI-NiI Complex Supported by a Terphenyl Diphosphine
• Authors of publication: Alexandra Velian; Sibo Lin; Alexander J. M. Miller; Michael W. Day; Theodor Agapie
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 6296 - 6297
• a: 11.7255 ± 0.0005 Å
• b: 13.1876 ± 0.0005 Å
• c: 14.7366 ± 0.0006 Å
• α: 105.066 ± 0.002°
• β: 97.41 ± 0.002°
• γ: 115.216 ± 0.002°
• Cell volume: 1914.32 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0569
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0565
• Weighted residual factors for all reflections included in the refinement: 0.0577
• Goodness-of-fit parameter for all reflections included in the refinement: 1.747
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No