Information card for entry 4102473

Structure parameters

• Formula: C68 H86 F6 N2 O12 S2 U
• Calculated formula: C68 H75 F6 N2 O12 S2 U
• Title of publication: Oxo Ligand Silylation in a Uranyl β-Ketoiminate Complex
• Authors of publication: Jessie L. Brown; Guang Wu; Trevor W. Hayton
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 7248 - 7249
• a: 15.8994 ± 0.001 Å
• b: 19.2681 ± 0.0013 Å
• c: 22.9828 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7040.8 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0942
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.1458
• Weighted residual factors for all reflections included in the refinement: 0.1612
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No