Information card for entry 4102507

Structure parameters

• Common name: ToMZnN(SiHMe2)2
• Chemical name: tris(4,4-dimethyl-2-oxazolinyl)phenylborato tetramethyldisilazato zinc
• Formula: C28.5 H47 B N4 O3 Si2 Zn
• Calculated formula: C28.5 H47 B N4 O3 Si2 Zn
• Title of publication: Conversion of a Zinc Disilazide to a Zinc Hydride Mediated by LiCl
• Authors of publication: Debabrata Mukherjee; Arkady Ellern; Aaron D. Sadow
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 7582 - 7583
• a: 9.9164 ± 0.0007 Å
• b: 15.0927 ± 0.001 Å
• c: 24.2345 ± 0.0016 Å
• α: 97.893 ± 0.001°
• β: 98.38 ± 0.001°
• γ: 106.934 ± 0.001°
• Cell volume: 3370.3 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.105
• Weighted residual factors for all reflections included in the refinement: 0.1161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No