Information card for entry 4102708

Structure parameters

• Formula: C57.5 H77.25 Cl2 N6 Si
• Calculated formula: C57.5 H77.16 Cl2 N6 Si
• Title of publication: A Facile Route to Functionalized N-Heterocyclic Carbenes (NHCs) with NHC Base-Stabilized Dichlorosilylene
• Authors of publication: Rajendra S. Ghadwal; Herbert W. Roesky; Markus Granitzka; Dietmar Stalke
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 10018 - 10020
• a: 11.9004 ± 0.0015 Å
• b: 15.3835 ± 0.0019 Å
• c: 15.9396 ± 0.0019 Å
• α: 76.172 ± 0.002°
• β: 73.774 ± 0.002°
• γ: 69.913 ± 0.002°
• Cell volume: 2598.1 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1069
• Residual factor for significantly intense reflections: 0.0615
• Weighted residual factors for significantly intense reflections: 0.1409
• Weighted residual factors for all reflections included in the refinement: 0.1631
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No