Information card for entry 4102774

Structure parameters

• Formula: C68 H52 B Cl F24 N2 Pd
• Calculated formula: C68 H52 B Cl F24 N2 Pd
• Title of publication: Palladium-Catalyzed Dimerization of Vinyl Ethers to Acetals
• Authors of publication: Changle Chen; Richard F. Jordan
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 10254 - 10255
• a: 13.226 ± 0.002 Å
• b: 14.275 ± 0.002 Å
• c: 18.644 ± 0.003 Å
• α: 82.897 ± 0.003°
• β: 84.533 ± 0.003°
• γ: 77.795 ± 0.002°
• Cell volume: 3405.4 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0861
• Residual factor for significantly intense reflections: 0.0648
• Weighted residual factors for significantly intense reflections: 0.1667
• Weighted residual factors for all reflections included in the refinement: 0.1777
• Goodness-of-fit parameter for all reflections included in the refinement: 0.932
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No