Information card for entry 4102941

Structure parameters

• Formula: C141 H240 Ir4 N8 P8
• Calculated formula: C141 H240 Ir4 N8 P8
• Title of publication: N-H Activation of Hydrazines by Iridium(I). Double N-H Activation To Form Iridium Aminonitrene Complexes
• Authors of publication: Zheng Huang; Jianrong (Steve) Zhou; John F. Hartwig
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 11458 - 11460
• a: 39.937 ± 0.006 Å
• b: 11.3904 ± 0.0015 Å
• c: 16.069 ± 0.002 Å
• α: 90°
• β: 94.863 ± 0.008°
• γ: 90°
• Cell volume: 7283.4 ± 1.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.15
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.0746
• Weighted residual factors for all reflections included in the refinement: 0.0933
• Goodness-of-fit parameter for all reflections included in the refinement: 0.922
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No