Information card for entry 4102961

Structure parameters

• Formula: C146 H153 Cl2 N10 Ni2 Pd
• Calculated formula: C146 H153 Cl2 N10 Ni2 Pd
• Title of publication: Directly Pd(II)-Bridged Porphyrin Belts with Remarkable Curvatures
• Authors of publication: Jianxin Song; Naoki Aratani; Ji Haeng Heo; Dongho Kim; Hiroshi Shinokubo; Atsuhiro Osuka
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 11868 - 11869
• a: 15.633 ± 0.002 Å
• b: 19.14 ± 0.002 Å
• c: 26.565 ± 0.003 Å
• α: 76.928 ± 0.002°
• β: 89.395 ± 0.002°
• γ: 72.777 ± 0.002°
• Cell volume: 7381.9 ± 1.5 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0891
• Residual factor for significantly intense reflections: 0.0744
• Weighted residual factors for significantly intense reflections: 0.2143
• Weighted residual factors for all reflections included in the refinement: 0.2279
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No