Information card for entry 4102969

Structure parameters

• Formula: C148 H170 B2 F48 Ni2 O3 P4 Si2
• Calculated formula: C148 H170 B2 F48 Ni2 O3 P4 Si2
• Title of publication: Arrested 1,2-Hydrogen Migration from Silicon to Nickel upon Oxidation of a Three-Coordinate Ni(I) Silyl Complex
• Authors of publication: Vlad M. Iluc; Gregory L. Hillhouse
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 11890 - 11892
• a: 14.5285 ± 0.0009 Å
• b: 16.1699 ± 0.001 Å
• c: 18.5044 ± 0.0011 Å
• α: 94.488 ± 0.001°
• β: 108.717 ± 0.001°
• γ: 106.896 ± 0.001°
• Cell volume: 3868.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0969
• Residual factor for significantly intense reflections: 0.0857
• Weighted residual factors for significantly intense reflections: 0.212
• Weighted residual factors for all reflections included in the refinement: 0.2227
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No