Information card for entry 4103057

Structure parameters

• Chemical name: Iron(IV) tetrakis(bistert-butyl ketimide)
• Formula: C36 H72 Fe N4
• Calculated formula: C36 H54 Fe N4
• Title of publication: Synthesis and Characterization of an Iron(IV) Ketimide Complex
• Authors of publication: Richard A. Lewis; Guang Wu; Trevor W. Hayton
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 12814 - 12816
• a: 22.138 ± 0.004 Å
• b: 8.5192 ± 0.0016 Å
• c: 22.613 ± 0.004 Å
• α: 90°
• β: 111.493 ± 0.003°
• γ: 90°
• Cell volume: 3968.2 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0962
• Residual factor for significantly intense reflections: 0.0716
• Weighted residual factors for significantly intense reflections: 0.1824
• Weighted residual factors for all reflections included in the refinement: 0.1989
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No