Information card for entry 4103142

Structure parameters

• Formula: C33 H55 B F4 N5 O P2 Rh
• Calculated formula: C33 H55 B F4 N5 O P2 Rh
• Title of publication: Intramolecular Hydroamination of Unbiased and Functionalized Primary Aminoalkenes Catalyzed by a Rhodium Aminophosphine Complex
• Authors of publication: Lisa D. Julian; John F. Hartwig
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 13813 - 13822
• a: 19.3079 ± 0.0012 Å
• b: 16.9887 ± 0.0011 Å
• c: 24.5185 ± 0.0017 Å
• α: 90°
• β: 104.227 ± 0.005°
• γ: 90°
• Cell volume: 7795.8 ± 0.9 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2036
• Residual factor for significantly intense reflections: 0.0762
• Weighted residual factors for significantly intense reflections: 0.1877
• Weighted residual factors for all reflections included in the refinement: 0.2532
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No