Information card for entry 4103205

Structure parameters

• Common name: {[SiP(Ph)3]Pt-Cl2CH2}{BArF}
• Formula: C45 H31 B0.5 Cl4 F12 P1.5 Pt0.5 Si0.5
• Calculated formula: C45 H31 B0.5 Cl4 F12 P1.5 Pt0.5 Si0.5
• Title of publication: Four-Coordinate, trigonal Pyramidal Pt(II) and Pd(II) Complexes
• Authors of publication: Charlene Tsay; Neal P. Mankad; Jonas C. Peters
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 13975 - 13977
• a: 12.6057 ± 0.0011 Å
• b: 17.5913 ± 0.0016 Å
• c: 20.2306 ± 0.0018 Å
• α: 84.459 ± 0.002°
• β: 84.435 ± 0.002°
• γ: 86.795 ± 0.002°
• Cell volume: 4439.2 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.084
• Residual factor for significantly intense reflections: 0.0635
• Weighted residual factors for significantly intense reflections: 0.16
• Weighted residual factors for all reflections included in the refinement: 0.1736
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No