Information card for entry 4103211

Structure parameters

• Common name: {[SiP(iPr)3]Pd}{BArF}
• Formula: C68 H66 B F24 P3 Pd Si
• Calculated formula: C68 H66 B F24 P3 Pd Si
• Title of publication: Four-Coordinate, trigonal Pyramidal Pt(II) and Pd(II) Complexes
• Authors of publication: Charlene Tsay; Neal P. Mankad; Jonas C. Peters
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 13975 - 13977
• a: 12.8728 ± 0.001 Å
• b: 38.131 ± 0.003 Å
• c: 14.4024 ± 0.0011 Å
• α: 90°
• β: 92.337 ± 0.001°
• γ: 90°
• Cell volume: 7063.6 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1419
• Weighted residual factors for all reflections included in the refinement: 0.1603
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No