Information card for entry 4103325

Structure parameters

• Common name: Pd-complex
• Chemical name: Pd-complex
• Formula: C27 H23 F6 N3 O8 Pd
• Calculated formula: C27 H23 F6 N3 O8 Pd
• Title of publication: Preparation and C-X Reductive Elimination Reactivity of Monoaryl PdIV-X Complexes in Water (X = OH, OH2, Cl, Br)
• Authors of publication: Williamson Oloo; Peter Y. Zavalij; Jing Zhang; Eugene Khaskin; Andrei N. Vedernikov
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 14400 - 14402
• a: 14.4824 ± 0.0012 Å
• b: 12.8318 ± 0.0011 Å
• c: 16.8071 ± 0.0014 Å
• α: 90°
• β: 113.782 ± 0.0013°
• γ: 90°
• Cell volume: 2858.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0414
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for significantly intense reflections: 0.0656
• Weighted residual factors for all reflections included in the refinement: 0.0681
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No