Information card for entry 4103400

Structure parameters

• Formula: C24 H18 Br4 N4 O6 Pd S
• Calculated formula: C24 H17.51 Br4 N4 O6 Pd S
• Title of publication: Synthesis of Metal-Hydrazone Complexes and Vapochromic Behavior of Their Hydrogen-Bonded Proton-Transfer Assemblies
• Authors of publication: Atsushi Kobayashi; Masa-aki Dosen; Mee Chang; Kiyohiko Nakajima; Shin-ichiro Noro; Masako Kato
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 15286 - 15298
• a: 13.98 ± 0.004 Å
• b: 4.8149 ± 0.0013 Å
• c: 42.22 ± 0.012 Å
• α: 90 ± 0.0007°
• β: 98.1321 ± 0.0008°
• γ: 90 ± 0.0007°
• Cell volume: 2813.3 ± 1.4 ų
• Cell temperature: 150.1 K
• Ambient diffraction temperature: 150.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for all reflections included in the refinement: 0.067
• Goodness-of-fit parameter for all reflections included in the refinement: 0.857
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No