Information card for entry 4103626

Structure parameters

• Chemical name: 1-(para-Bromophenyl)-1,2,2-(2',4',6'-triisopropylphenyl)disilene
• Formula: C51 H73 Br Si2
• Calculated formula: C51 H73 Br Si2
• Title of publication: Transfer of a Disilenyl Moiety to Aromatic Substrates and Lateral Functional Group Transformation in Aryl Disilenes
• Authors of publication: Jonathan Jeck; Iulia Bejan; Andrew J. P. White; Dominik Nied; Frank Breher; David Scheschkewitz
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 17306 - 17315
• a: 18.5602 ± 0.0003 Å
• b: 12.8496 ± 0.00016 Å
• c: 21.6993 ± 0.0003 Å
• α: 90°
• β: 109.514 ± 0.0016°
• γ: 90°
• Cell volume: 4877.84 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0712
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0895
• Goodness-of-fit parameter for all reflections included in the refinement: 0.909
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No