Crystallography Open Database

Information card for entry 4103718

Preview

Coordinates	4103718.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H72 N4 W
Calculated formula	C36 H72 N4 W
Title of publication	Diamagnetic Group 6 Tetrakis(di-tert-butylketimido)metal(IV) Complexes
Authors of publication	Rosanna A. D. Soriaga; Jennifer M. Nguyen; Thomas A. Albright; David M. Hoffman
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	18014 - 18016
a	15.4819 ± 0.0007 Å
b	16.6244 ± 0.0008 Å
c	15.6247 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	4021.4 ± 0.3 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	4
Space group number	63
Hermann-Mauguin space group symbol	C m c m
Hall space group symbol	-C 2c 2
Residual factor for all reflections	0.0205
Residual factor for significantly intense reflections	0.0194
Weighted residual factors for significantly intense reflections	0.0507
Weighted residual factors for all reflections included in the refinement	0.0516
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4103718.html