Information card for entry 4103799

Structure parameters

• Formula: C99.5 H112 B6 P6 S6 U3
• Calculated formula: C99.5 H108 B6 P6 S6 U3
• Title of publication: The U=C Double Bond: Synthesis and Study of Uranium Nucleophilic Carbene Complexes
• Authors of publication: Thibault Cantat; Thérèse Arliguie; Anne Noël; Pierre Thuéry; Michel Ephritikhine; Pascal Le Floch; Nicolas Mézailles
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 963 - 972
• a: 14.0685 ± 0.0003 Å
• b: 15.4706 ± 0.0003 Å
• c: 24.6002 ± 0.0004 Å
• α: 107.317 ± 0.002°
• β: 98.742 ± 0.001°
• γ: 95.683 ± 0.001°
• Cell volume: 4992.72 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0525
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.076
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No