Information card for entry 4103829

Structure parameters

• Formula: C35 H48 Ge N2 O4
• Calculated formula: C35 H48 Ge N2 O4
• SMILES: [Ge]1(N(c2c(C(C)C)cccc2C(C)C)C(=CC(=[N]1c1c(C(C)C)cccc1C(C)C)C)C)/C(=C\C(=O)OC)C(=O)OC
• Title of publication: A Germanium(II) Hydride as an Effective Reagent for Hydrogermylation Reactions
• Authors of publication: Anukul Jana; Debajyoti Ghoshal; Herbert W. Roesky; Ina Objartel; Gerald Schwab; Dietmar Stalke
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 1288 - 1293
• a: 12.0106 ± 0.0019 Å
• b: 15.01 ± 0.002 Å
• c: 19.635 ± 0.003 Å
• α: 90°
• β: 103.98 ± 0.002°
• γ: 90°
• Cell volume: 3434.9 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for significantly intense reflections: 0.0649
• Weighted residual factors for all reflections included in the refinement: 0.0668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No