Information card for entry 4103840

Structure parameters

• Formula: C192 H144 N32 O8 Os8
• Calculated formula: C192 H144 N32 O8 Os8
• Title of publication: Regioselective Knitting of Anilinevia ortho-C-N Bond Fusion Using OsO4 as a Template
• Authors of publication: Subhas Samanta; Sreebrata Goswami
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 924 - 925
• a: 26.657 ± 0.005 Å
• b: 9.5372 ± 0.0017 Å
• c: 16.013 ± 0.003 Å
• α: 90°
• β: 106.516 ± 0.003°
• γ: 90°
• Cell volume: 3903.1 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for significantly intense reflections: 0.1045
• Weighted residual factors for all reflections included in the refinement: 0.114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.172
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No