Information card for entry 4103934

Structure parameters

• Formula: C24 H32 O3
• Calculated formula: C24 H32 O3
• Title of publication: Stereocontrolled Synthesis of Complicated Oxacyclic Compounds via Platinum-Catalyzed [4 + 2]-Cycloadditions and Annulations of Enynals with Allylic Alcohols
• Authors of publication: Yu-Chia Hsu; Chun-Ming Ting; Rai-Shung Liu
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 2090 - 2091
• a: 6.1427 ± 0.0002 Å
• b: 12.2134 ± 0.0006 Å
• c: 27.1155 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2034.29 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1023
• Residual factor for significantly intense reflections: 0.0876
• Weighted residual factors for significantly intense reflections: 0.2395
• Weighted residual factors for all reflections included in the refinement: 0.2544
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No