Crystallography Open Database

Information card for entry 4104044

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Coordinates	4104044.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H26 Cl2 F2 N2 Pd
Calculated formula	C19 H26 Cl2 F2 N2 Pd
Title of publication	Synthesis and Reactivity of a Mono-σ-Aryl Palladium(IV) Fluoride Complex
Authors of publication	Nicholas D. Ball; Melanie S. Sanford
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	3796 - 3797
a	11.1616 ± 0.0009 Å
b	11.9919 ± 0.0009 Å
c	15.6096 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	2089.3 ± 0.3 Å³
Cell temperature	85 ± 2 K
Ambient diffraction temperature	85 ± 2 K
Number of distinct elements	6
Space group number	56
Hermann-Mauguin space group symbol	P c c n
Hall space group symbol	-P 2ab 2ac
Residual factor for all reflections	0.0507
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.1032
Weighted residual factors for all reflections included in the refinement	0.1102
Goodness-of-fit parameter for all reflections included in the refinement	1.095
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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