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Information card for entry 4104071
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Coordinates | 4104071.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | tris((2'-phenylcarboxy-1,1'-(S)binaphthalen-2-yl)-oxy)phosphine dichloromethane solute |
---|---|
Formula | C82 H53 Cl2 O9 P |
Calculated formula | C81 H51 Cl1.995 O9 P |
Title of publication | Helical Triskelion Monophosphites as Ligands in Asymmetric Catalysis |
Authors of publication | Manfred T. Reetz; Hongchao Guo; Jun-An Ma; Richard Goddard; Richard J. Mynott |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 4136 - 4142 |
a | 20.6143 ± 0.0002 Å |
b | 20.6143 ± 0.0002 Å |
c | 17.9025 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 6588.42 ± 0.14 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 5 |
Space group number | 173 |
Hermann-Mauguin space group symbol | P 63 |
Hall space group symbol | P 6c |
Residual factor for all reflections | 0.0966 |
Residual factor for significantly intense reflections | 0.0765 |
Weighted residual factors for significantly intense reflections | 0.1671 |
Weighted residual factors for all reflections included in the refinement | 0.1784 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.077 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4104071.html
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