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Information card for entry 4104091
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Coordinates | 4104091.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H64 N2 O7 Ru |
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Calculated formula | C41 H52 N2 O7 Ru |
Title of publication | cis-β-Bis(carbonyl) Ruthenium-Salen Complexes: X-ray Crystal Structures and Remarkable Catalytic Properties toward Asymmetric Intramolecular Alkene Cyclopropanation |
Authors of publication | Zhen-Jiang Xu; Ran Fang; Cunyuan Zhao; Jie-Sheng Huang; Gong-Yong Li; Nianyong Zhu; Chi-Ming Che |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 4405 - 4417 |
a | 9.439 ± 0.0019 Å |
b | 17.257 ± 0.004 Å |
c | 13.365 ± 0.003 Å |
α | 90° |
β | 93.96 ± 0.03° |
γ | 90° |
Cell volume | 2171.8 ± 0.8 Å3 |
Cell temperature | 301 ± 2 K |
Ambient diffraction temperature | 301 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0731 |
Residual factor for significantly intense reflections | 0.0497 |
Weighted residual factors for significantly intense reflections | 0.1118 |
Weighted residual factors for all reflections included in the refinement | 0.1194 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.816 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4104091.html
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