Information card for entry 4104106

Structure parameters

• Formula: C37 H30 F3 P2 Rh
• Calculated formula: C37 H30 F3 P2 Rh
• Title of publication: Fluxionality of [(Ph3P)3Rh(X)]: The Extreme Case of X = CF3
• Authors of publication: Jenni Goodman; Vladimir V. Grushin; Roman B. Larichev; Stuart A. Macgregor; William J. Marshall; D. Christopher Roe
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 4236 - 4238
• a: 9.1363 ± 0.0005 Å
• b: 37.72 ± 0.002 Å
• c: 9.7614 ± 0.0006 Å
• α: 90°
• β: 110.106 ± 0.001°
• γ: 90°
• Cell volume: 3159 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0996
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.0992
• Weighted residual factors for all reflections included in the refinement: 0.1189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No