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Information card for entry 4104146
Preview
Coordinates | 4104146.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H43 N3 Si |
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Calculated formula | C29 H43 N3 Si |
SMILES | [SiH]1(N)N(c2c(cccc2C(C)C)C(C)C)C(=CC(=C)N1c1c(cccc1C(C)C)C(C)C)C |
Title of publication | Oxidative Addition of Ammonia at a Silicon(II) Center and an Unprecedented Hydrogenation Reaction of Compounds with Low-Valent Group 14 Elements Using Ammonia Borane |
Authors of publication | Anukul Jana; Carola Schulzke; Herbert W. Roesky |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 4600 - 4601 |
a | 15.529 ± 0.003 Å |
b | 17.296 ± 0.004 Å |
c | 20.897 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5613 ± 2 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 4 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0782 |
Residual factor for significantly intense reflections | 0.0625 |
Weighted residual factors for significantly intense reflections | 0.1443 |
Weighted residual factors for all reflections included in the refinement | 0.1523 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.112 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4104146.html
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