Information card for entry 4104182

Structure parameters

• Formula: C24 H20 Al As Cl5 Sb
• Calculated formula: C24 H20 Al As Cl5 Sb
• SMILES: [Sb]([As](c1ccccc1)(c1ccccc1)c1ccccc1)(Cl)c1ccccc1.[Cl-][Al](Cl)(Cl)Cl
• Title of publication: Coordination of Arsine Ligands as a General Synthetic Approach to Rare Examples of Arsenic-Antimony and Arsenic-Bismuth Bonds
• Authors of publication: Eamonn Conrad; Neil R. Burford; Robert McDonald; Michael J. Ferguson
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 5066 - 5067
• a: 31.0351 ± 0.0019 Å
• b: 11.9521 ± 0.0007 Å
• c: 15.0928 ± 0.0009 Å
• α: 90°
• β: 99.7641 ± 0.0009°
• γ: 90°
• Cell volume: 5517.3 ± 0.6 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0394
• Residual factor for significantly intense reflections: 0.0286
• Weighted residual factors for significantly intense reflections: 0.0701
• Weighted residual factors for all reflections included in the refinement: 0.0813
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No