Information card for entry 4104608

Structure parameters

• Formula: C92 H40 B5 F60 K N4 O4
• Calculated formula: C92 H40 B5 F60 K N4 O4
• Title of publication: Synthesis, Structure, and Bonding of Weakly Coordinating Anions Based on CN Adducts
• Authors of publication: Arne Bernsdorf; Harald Brand; Robert Hellmann; Martin Köckerling; Axel Schulz; Alexander Villinger; Karsten Voss
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 8958 - 8970
• a: 17.9158 ± 0.0005 Å
• b: 18.8215 ± 0.0006 Å
• c: 21.0662 ± 0.0006 Å
• α: 111.374 ± 0.002°
• β: 111.849 ± 0.002°
• γ: 112.211 ± 0.002°
• Cell volume: 4938 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0866
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1161
• Weighted residual factors for all reflections included in the refinement: 0.1292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No