Information card for entry 4104632

Structure parameters

• Common name: iPr3SiPPMo(N[tBu]Ar)3
• Formula: C48 H82 Mo N3 P2 Si
• Calculated formula: C48 H82 Mo N3 P2 Si
• Title of publication: An Unusual P-P Double Bond Formed via Phospha-Wittig Transformation of a Terminal PO Complex
• Authors of publication: Nicholas A. Piro; Christopher C. Cummins
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 8764 - 8765
• a: 11.4081 ± 0.001 Å
• b: 15.4385 ± 0.0014 Å
• c: 16.768 ± 0.0015 Å
• α: 65.237 ± 0.001°
• β: 72.983 ± 0.002°
• γ: 75.312 ± 0.002°
• Cell volume: 2534.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0528
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0734
• Weighted residual factors for all reflections included in the refinement: 0.0816
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No