Information card for entry 4104638

Structure parameters

• Formula: C31 H38 Mo O3 Si
• Calculated formula: C31 H38 Mo O3 Si
• Title of publication: η3-Silapropargyl/Alkynylsilyl Molybdenum Complexes: Synthesis, Structure, and Reactivity toward Methanol
• Authors of publication: Mako Yabe-Yoshida; Chizuko Kabuto; Kuninobu Kabuto; Eunsang Kwon; Hiroyuki Sakaba
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 9138 - 9139
• a: 11.3091 ± 0.0008 Å
• b: 14.9091 ± 0.0011 Å
• c: 18.1392 ± 0.0011 Å
• α: 100 ± 0.003°
• β: 96.53 ± 0.003°
• γ: 99.907 ± 0.003°
• Cell volume: 2934.4 ± 0.4 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for all reflections included in the refinement: 0.1834
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No