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Information card for entry 4104771
Preview
Coordinates | 4104771.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H21 N O3 |
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Calculated formula | C23 H21 N O3 |
SMILES | O1C(N(C(Cc2ccccc2)C1=O)C(=O)c1c2ccccc2ccc1)(C)C |
Title of publication | Memory of Chirality of Tertiary Aromatic Amides: A Simple and Efficient Method for the Enantioselective Synthesis of Quaternary α-Amino Acids |
Authors of publication | Mathieu Branca; Sébastien Pena; Régis Guillot; Didier Gori; Valérie Alezra; Cyrille Kouklovsky |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 10711 - 10718 |
a | 7.713 ± 0.005 Å |
b | 14.863 ± 0.005 Å |
c | 31.233 ± 0.005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3580 ± 3 Å3 |
Cell temperature | 100 ± 1 K |
Ambient diffraction temperature | 100 ± 1 K |
Number of distinct elements | 4 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0969 |
Residual factor for significantly intense reflections | 0.0781 |
Weighted residual factors for significantly intense reflections | 0.192 |
Weighted residual factors for all reflections included in the refinement | 0.1995 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.172 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4104771.html
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