Information card for entry 4104779

Structure parameters

• Formula: C32 H40 F6 Mo N2 O
• Calculated formula: C32 H40 F6 Mo N2 O
• Title of publication: Endo-Selective Enyne Ring-Closing Metathesis Promoted by Stereogenic-at-Mo Monoalkoxide and Monoaryloxide Complexes. Efficient Synthesis of Cyclic Dienes Not Accessible through Reactions with Ru Carbenes
• Authors of publication: Yeon-Ju Lee; Richard R. Schrock; Amir H. Hoveyda
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 10652 - 10661
• a: 10.7606 ± 0.0018 Å
• b: 14.085 ± 0.002 Å
• c: 21.094 ± 0.004 Å
• α: 90.729 ± 0.002°
• β: 90.393 ± 0.002°
• γ: 95.057 ± 0.002°
• Cell volume: 3184.3 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0716
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No