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Information card for entry 4104821
Preview
Coordinates | 4104821.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C35.5 H92 K N6 O2 Si8 Y2 |
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Calculated formula | C35.5 H88 K N6 O2 Si8 Y2 |
Title of publication | Isolation of Dysprosium and Yttrium Complexes of a Three-Electron Reduction Product in the Activation of Dinitrogen, the (N2)3- Radical |
Authors of publication | William J. Evans; Ming Fang; Gaël Zucchi; Filipp Furche; Joseph W. Ziller; Ryan M. Hoekstra; Jeffrey I. Zink |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 11195 - 11202 |
a | 12.481 ± 0.003 Å |
b | 21.371 ± 0.005 Å |
c | 22.304 ± 0.005 Å |
α | 90° |
β | 105.071 ± 0.003° |
γ | 90° |
Cell volume | 5745 ± 2 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0646 |
Residual factor for significantly intense reflections | 0.0372 |
Weighted residual factors for significantly intense reflections | 0.0808 |
Weighted residual factors for all reflections included in the refinement | 0.091 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.015 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4104821.html
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