Crystallography Open Database

Information card for entry 4105092

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Coordinates	4105092.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	JLG-12
Formula	C180 H600 Ge139.73 N60 O339.45
Calculated formula	Ge139.728 O339.456
Title of publication	A Crystalline Germanate with Mesoporous 30-Ring Channels
Authors of publication	Xiaoyan Ren; Yi Li; Qinhe Pan; Jihong Yu; Ruren Xu; Ying Xu
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	14128 - 14129
a	46.377 ± 0.009 Å
b	26.689 ± 0.005 Å
c	12.107 ± 0.002 Å
α	90°
β	92.84 ± 0.03°
γ	90°
Cell volume	14967 ± 5 Å³
Cell temperature	4 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.1436
Residual factor for significantly intense reflections	0.0938
Weighted residual factors for significantly intense reflections	0.2237
Weighted residual factors for all reflections included in the refinement	0.2436
Goodness-of-fit parameter for all reflections included in the refinement	0.907
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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