Crystallography Open Database

Information card for entry 4105105

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Coordinates	4105105.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H37 P4 Rh S
Calculated formula	C18 H37 P4 Rh S
Title of publication	Thermodynamic Studies and Hydride Transfer Reactions from a Rhodium Complex to BX3 Compounds
Authors of publication	Michael T. Mock; Robert G. Potter; Donald M. Camaioni; Jun Li; William G. Dougherty; W. Scott Kassel; Brendan Twamley; Daniel L. DuBois
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	14454 - 14465
a	30.0678 ± 0.0005 Å
b	9.3277 ± 0.0001 Å
c	17.4534 ± 0.0003 Å
α	90°
β	100.997 ± 0.001°
γ	90°
Cell volume	4805.15 ± 0.13 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0242
Residual factor for significantly intense reflections	0.0225
Weighted residual factors for significantly intense reflections	0.0588
Weighted residual factors for all reflections included in the refinement	0.0598
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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