Information card for entry 4105119

Structure parameters

• Formula: C84.5 H102 Ge2 O4
• Calculated formula: C84.5 H102 Ge2 O4
• Title of publication: An Unsymmetric Oxo/Imido-Bridged Germanium-Centered Singlet Diradicaloid
• Authors of publication: Xinping Wang; Yang Peng; Marilyn M. Olmstead; James C. Fettinger; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 14164 - 14165
• a: 16.33 ± 0.003 Å
• b: 16.55 ± 0.003 Å
• c: 27.623 ± 0.005 Å
• α: 90°
• β: 105.873 ± 0.003°
• γ: 90°
• Cell volume: 7181 ± 2 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1158
• Residual factor for significantly intense reflections: 0.0924
• Weighted residual factors for significantly intense reflections: 0.2316
• Weighted residual factors for all reflections included in the refinement: 0.242
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No