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Information card for entry 4105186
Preview
Coordinates | 4105186.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C62 H70 B F26 P2 Rh |
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Calculated formula | C62 H70 B F26 P2 Rh |
Title of publication | Monomeric and Oligomeric Amine-Borane σ-Complexes of Rhodium. Intermediates in the Catalytic Dehydrogenation of Amine-Boranes |
Authors of publication | Thomas M. Douglas; Adrian B. Chaplin; Andrew S. Weller; Xinzheng Yang; Michael B. Hall |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 15440 - 15456 |
a | 21.7964 ± 0.0002 Å |
b | 13.1712 ± 0.0002 Å |
c | 25.5387 ± 0.0003 Å |
α | 90° |
β | 113.759 ± 0.0005° |
γ | 90° |
Cell volume | 6710.37 ± 0.15 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1291 |
Residual factor for significantly intense reflections | 0.0906 |
Weighted residual factors for significantly intense reflections | 0.2499 |
Weighted residual factors for all reflections included in the refinement | 0.2825 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105186.html
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