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Information card for entry 4105350
Preview
Coordinates | 4105350.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C56 H42 Br16 N4 O18 Rh2 |
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Calculated formula | C56 H42 Br16 N4 O18 Rh2 |
Title of publication | Experimental Evidence for the All-Up Reactive Conformation of Chiral Rhodium(II) Carboxylate Catalysts: Enantioselective Synthesis of cis-Cyclopropane α-Amino Acids |
Authors of publication | Vincent N. G. Lindsay; Wei Lin; André B. Charette |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 16383 - 16385 |
a | 19.177 ± 0.0003 Å |
b | 22.7929 ± 0.0003 Å |
c | 23.4525 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 10251.1 ± 0.2 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 6 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0559 |
Residual factor for significantly intense reflections | 0.0381 |
Weighted residual factors for significantly intense reflections | 0.0812 |
Weighted residual factors for all reflections included in the refinement | 0.0839 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105350.html
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Users of the data should acknowledge the original authors of the
structural data.