Information card for entry 4105379

Structure parameters

• Formula: C48 H40 Al2 As2 Cl8 P2
• Calculated formula: C48 H40 Al2 As2 Cl8 P2
• Title of publication: Phosphinopnictonium Cations: High Yield and General Preparative Procedures for New Interpnictogen Frameworks Exploiting As→P and Sb→P Coordinate Bonds
• Authors of publication: Eamonn Conrad; Neil Burford; Robert McDonald; Michael J. Ferguson
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17000 - 17008
• a: 11.327 ± 0.003 Å
• b: 11.345 ± 0.003 Å
• c: 20.433 ± 0.006 Å
• α: 90.271 ± 0.004°
• β: 98.929 ± 0.004°
• γ: 90.595 ± 0.004°
• Cell volume: 2593.7 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1012
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for significantly intense reflections: 0.2232
• Weighted residual factors for all reflections included in the refinement: 0.2448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No