Information card for entry 4105397

Structure parameters

• Chemical name: catena-{(μ2-Chloro)-(μ2-dioxane-O,O')-lithium(i)}
• Formula: C4 H8 Cl Li O2
• Calculated formula: C4 H8 Cl Li O2
• Title of publication: Revelation of the Difference between Arylzinc Reagents Prepared from Aryl Grignard and Aryllithium Reagents Respectively: Kinetic and Structural Features
• Authors of publication: Liqun Jin; Chao Liu; Jing Liu; Fang Hu; Yu Lan; Andrei S. Batsanov; Judith A. K. Howard; Todd B. Marder; Aiwen Lei
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 16656 - 16657
• a: 7.1229 ± 0.0004 Å
• b: 7.75 ± 0.0004 Å
• c: 11.403 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 629.47 ± 0.06 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0211
• Residual factor for significantly intense reflections: 0.0201
• Weighted residual factors for significantly intense reflections: 0.0518
• Weighted residual factors for all reflections included in the refinement: 0.0523
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No