Information card for entry 4105409

Structure parameters

• Formula: C41 H69 N4 U
• Calculated formula: C41 H69 N4 U
• Title of publication: Synthesis of Heteroleptic Uranium (μ-η6:η6-C6H6)2- Sandwich Complexes via Facile Displacement of (η5-C5Me5)1- by Ligands of Lower Hapticity and Their Conversion to Heteroleptic Bis(imido) Compounds
• Authors of publication: William J. Evans; Christopher A. Traina; Joseph W. Ziller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17473 - 17481
• a: 9.938 ± 0.0007 Å
• b: 10.8469 ± 0.0008 Å
• c: 20.2681 ± 0.0019 Å
• α: 92.82 ± 0.001°
• β: 91.435 ± 0.001°
• γ: 116.534 ± 0.001°
• Cell volume: 1949.6 ± 0.3 ų
• Cell temperature: 148 ± 2 K
• Ambient diffraction temperature: 148 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0169
• Residual factor for significantly intense reflections: 0.0159
• Weighted residual factors for significantly intense reflections: 0.0389
• Weighted residual factors for all reflections included in the refinement: 0.0393
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No