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Information card for entry 4105411
Preview
Coordinates | 4105411.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C47 H79 N5 Si2 U |
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Calculated formula | C47 H79 N5 Si2 U |
Title of publication | Synthesis of Heteroleptic Uranium (μ-η6:η6-C6H6)2- Sandwich Complexes via Facile Displacement of (η5-C5Me5)1- by Ligands of Lower Hapticity and Their Conversion to Heteroleptic Bis(imido) Compounds |
Authors of publication | William J. Evans; Christopher A. Traina; Joseph W. Ziller |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2009 |
Journal volume | 131 |
Pages of publication | 17473 - 17481 |
a | 13.5148 ± 0.0007 Å |
b | 18.2529 ± 0.0009 Å |
c | 19.2967 ± 0.001 Å |
α | 90° |
β | 90.0839 ± 0.0007° |
γ | 90° |
Cell volume | 4760.2 ± 0.4 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0637 |
Residual factor for significantly intense reflections | 0.0452 |
Weighted residual factors for significantly intense reflections | 0.1052 |
Weighted residual factors for all reflections included in the refinement | 0.1128 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105411.html
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