Information card for entry 4105413

Structure parameters

• Formula: C22 H54 Li2 N4 Si2
• Calculated formula: C22 H54 Li2 N4 Si2
• Title of publication: Low-Temperature Addition of Organolithiums to Functionalized Vinylsilanes under Formation of Secondary α-Lithiated Alkylsilanes
• Authors of publication: Christian Unkelbach; Carsten Strohmann
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17044 - 17045
• a: 9.562 ± 0.005 Å
• b: 10.587 ± 0.004 Å
• c: 15.491 ± 0.007 Å
• α: 96.133 ± 0.006°
• β: 107.6 ± 0.005°
• γ: 90.475 ± 0.009°
• Cell volume: 1484.9 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0633
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.1404
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No