Information card for entry 4105449

Structure parameters

• Formula: C24 H44 Cl5 Ga P4
• Calculated formula: C24 H44 Cl5 Ga P4
• SMILES: [Ga](Cl)(Cl)([Cl-])Cl.Cl[P+]1(P(P(P1C1CCCCC1)C1CCCCC1)C1CCCCC1)C1CCCCC1
• Title of publication: New Synthetic Procedures to Catena-Phosphorus Cations: Preparation and Dissociation of the First cyclo-Phosphino-halophosphonium Salts
• Authors of publication: Jan J. Weigand; Neil Burford; Reagan J. Davidson; T. Stanley Cameron; Patrick Seelheim
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17943 - 17953
• a: 18.491 ± 0.009 Å
• b: 9.143 ± 0.009 Å
• c: 19.97 ± 0.005 Å
• α: 90°
• β: 104.27 ± 0.05°
• γ: 90°
• Cell volume: 3272 ± 4 ų
• Cell temperature: 123.1 K
• Ambient diffraction temperature: 123.1 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for all reflections included in the refinement: 0.0589
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No