Information card for entry 4105460

Structure parameters

• Common name: {[Me2NN]Cu}2(m-h2:h1-ONAr) + 0.5 ether
• Formula: C52 H64 Cu2 N5 O1.5
• Calculated formula: C52 H64 Cu2 N5 O1.5
• Title of publication: Nitric Oxide Oxidatively Nitrosylates Ni(I) and Cu(I) C-Organonitroso Adducts
• Authors of publication: Stefan Wiese; Pooja Kapoor; Kamille D. Williams; Timothy H. Warren
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 18105 - 18111
• a: 35.714 ± 0.011 Å
• b: 11.67 ± 0.002 Å
• c: 23.333 ± 0.005 Å
• α: 90°
• β: 93.64 ± 0.02°
• γ: 90°
• Cell volume: 9705 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1281
• Residual factor for significantly intense reflections: 0.0832
• Weighted residual factors for significantly intense reflections: 0.1881
• Weighted residual factors for all reflections included in the refinement: 0.2053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No