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Information card for entry 4105528
Preview
Coordinates | 4105528.cif |
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Original paper (by DOI) | HTML |
Formula | C32 H43 N O4 Si |
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Calculated formula | C32 H43 N O4 Si |
SMILES | [Si]1(O[C@@H]([C@H](C(=CC=C(O1)N1C(=O)OC[C@@H]1Cc1ccccc1)C)C)c1ccccc1)(C(C)(C)C)C(C)(C)C |
Title of publication | Silylene-Mediated Polarity Reversal of Dienoates: Additions of Dienoates to Aldehydes at the δ-Position To Form trans-Dioxasilacyclononenes |
Authors of publication | Christian C. Ventocilla; K. A. Woerpel |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 406 - 408 |
a | 9.0489 ± 0.0009 Å |
b | 11.8543 ± 0.0012 Å |
c | 14.1652 ± 0.0014 Å |
α | 96.5484 ± 0.0012° |
β | 99.1573 ± 0.0012° |
γ | 90.8419 ± 0.0012° |
Cell volume | 1489.5 ± 0.3 Å3 |
Cell temperature | 143 ± 2 K |
Ambient diffraction temperature | 143 ± 2 K |
Number of distinct elements | 5 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0424 |
Residual factor for significantly intense reflections | 0.0391 |
Weighted residual factors for significantly intense reflections | 0.1009 |
Weighted residual factors for all reflections included in the refinement | 0.1037 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4105528.html
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