Information card for entry 4105651

Structure parameters

• Formula: C41.25 H62 B N2 O2 Os P2
• Calculated formula: C41.25 H62 B N2 O2 Os P2
• Title of publication: From Tetrahydroborate- to Aminoborylvinylidene-Osmium Complexes via Alkynyl-Aminoboryl Intermediates
• Authors of publication: María L. Buil; Miguel A. Esteruelas; Karin Garcés; Enrique Oñate
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 2250 - 2263
• a: 10.7453 ± 0.0009 Å
• b: 13.0951 ± 0.001 Å
• c: 16.1287 ± 0.0014 Å
• α: 86.901 ± 0.002°
• β: 82.155 ± 0.002°
• γ: 67.312 ± 0.003°
• Cell volume: 2074.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0404
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0862
• Weighted residual factors for all reflections included in the refinement: 0.0899
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No