Information card for entry 4105655

Structure parameters

• Formula: C42 H63 B N2 O2 Os P2
• Calculated formula: C42 H63 B N2 O2 Os P2
• Title of publication: From Tetrahydroborate- to Aminoborylvinylidene-Osmium Complexes via Alkynyl-Aminoboryl Intermediates
• Authors of publication: María L. Buil; Miguel A. Esteruelas; Karin Garcés; Enrique Oñate
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 2250 - 2263
• a: 10.5199 ± 0.0001 Å
• b: 14.3046 ± 0.0004 Å
• c: 15.6759 ± 0.0004 Å
• α: 107.045 ± 0.002°
• β: 104.592 ± 0.0019°
• γ: 104.807 ± 0.002°
• Cell volume: 2039.57 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.042
• Residual factor for significantly intense reflections: 0.0277
• Weighted residual factors for significantly intense reflections: 0.0475
• Weighted residual factors for all reflections included in the refinement: 0.0491
• Goodness-of-fit parameter for all reflections included in the refinement: 0.908
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No