Crystallography Open Database

Information card for entry 4105670

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Coordinates	4105670.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H55 F6 N2 P Rh Sb
Calculated formula	C43 H55 F6 N2 P Rh Sb
Title of publication	Rhodium Phosphine-π-Arene Intermediates in the Hydroamination of Alkenes
Authors of publication	Zhijian Liu; Hideaki Yamamichi; Sherzod T. Madrahimov; John F. Hartwig
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	2772 - 2782
a	9.3718 ± 0.0012 Å
b	15.838 ± 0.002 Å
c	14.0215 ± 0.0018 Å
α	90°
β	98.362 ± 0.009°
γ	90°
Cell volume	2059.1 ± 0.5 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1094
Residual factor for significantly intense reflections	0.0573
Weighted residual factors for significantly intense reflections	0.0911
Weighted residual factors for all reflections included in the refinement	0.1061
Goodness-of-fit parameter for all reflections included in the refinement	0.993
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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