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Information card for entry 4105703
Preview
Coordinates | 4105703.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H38 B2 Cl4 F8 Ni P2 S2 |
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Calculated formula | C32 H38 B2 Cl4 F8 Ni P2 S2 |
Title of publication | Plasticity of the Nickel(II) Coordination Environment in Complexes with Hemilabile Phosphino Thioether Ligands |
Authors of publication | Charles W. Machan; Alexander M. Spokoyny; Matthew R. Jones; Amy A. Sarjeant; Charlotte L. Stern; Chad A. Mirkin |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2011 |
Journal volume | 133 |
Pages of publication | 3023 - 3033 |
a | 13.2709 ± 0.0006 Å |
b | 14.7678 ± 0.0009 Å |
c | 23.4392 ± 0.0013 Å |
α | 89.618 ± 0.004° |
β | 74.335 ± 0.003° |
γ | 65.263 ± 0.003° |
Cell volume | 3987.4 ± 0.4 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1379 |
Residual factor for significantly intense reflections | 0.0744 |
Weighted residual factors for significantly intense reflections | 0.2034 |
Weighted residual factors for all reflections included in the refinement | 0.2393 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.988 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4105703.html
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structural data.